Amazing Spider-Man Vol.1 #88
From his prison cell, Doc Ock calls to his mechanical arms and even Spidey can't stop the inevitable reuinion; Ock hijacks a plane and holds an Asian general hostage for ten million bucks but Spidey foils his plans.
Printed: Sept 1970
Writers: Stan Lee
Art: John Romita Sr. and Jim Mooney
Cover: John Romita Sr.