Amazing Spider-Man Vol.1 #52
The Kingpin has an unconscious Spidey and J. Jonah Jameson sealed up tight in a watery deathtrap!; If they want to get out while still breathing, Jameson will have to wake Spider-Man up from his afternoon nap.
Printed: Sept 1967
Writers: Stan Lee
Art: John Romita Sr. and Mike Esposito [Mickey Dimeo]
Cover: John Romita Sr.